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Research article
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Preparation and characterization of electrospun fibers of Nylon 11
M. Dhanalakshmi, J. P. Jog
Vol. 2., No.8., Pages 540-545, 2008
DOI: 10.3144/expresspolymlett.2008.65
Corresponding author: J. P. Jog

GRAPHICAL ABSTRACT

ABSTRACT

Nylon 11 nanofibers mats were successfully prepared by electrospinning process from formic acid solution. The scanning electron microscopy (SEM) images showed that nanofibers with uniform diameter were produced when the polymer concentration was 10% w/v, whereas ribbons were formed at a higher concentration. The crystalline structure of the nanofibers mats was investigated using X-ray diffraction (XRD) and it was found that the nanofibers mats crystallized in α form. The melt crystallized as well as solution casted films however exhibited γ form. The thermal properties of these samples were studied using differential scanning calorimetry (DSC) and it was observed that electrospun fibers showed higher crystallinity than the melt-crystallized samples. However, the crystallinity of electrospun fibers was lower than the solution-crystallized sample.
Published by:

Budapest University of Technology and Economics,
Faculty of Mechanical Engineering, Department of Polymer Engineering